Dapsone_LCMS_16760_MedChemExpress

Data File D:\\AGLIENT 1260\\DATA\\20150629\\20150629 2015-06-29 09-33-24\\BIZ2015-629-DJL4.DSample Name: BIZ2015-629-DJL4=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 35Acq. Instrument : HY-LCMS-02 Location : P1-D-03Injection Date : 6/29/2015 1:49:17 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150629\\20150629 2015-06-29 09-33-24\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 6/29/2015 9:33:24 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\10-80A,15MIN(RP-HPLC).MLast changed : 6/29/2015 2:15:15 PM by Li Shan(LCMS-02) (modified after loading)Method Info : 10-80A,16MIN Catalog No : HY-B0688 Batch#16760 A-RP-132 Additional Info : Peak(s) manually integrated DAD1 C, Sig=254,4 Ref=off (D:\\AGLIENT...60\\DATA\\20150629\\20150629 2015-06-29 09-33-24\\BIZ2015-629-DJL4.D) 1.671mAU20001500100050000.51 1.955 1.560 2.1701.522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 C, Sig=254,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.560 MM 0.0559 2.16334 6.45028e-1 0.0301 2 1.671 MM 0.0498 7143.93311 2391.50000 99.4547 3 1.955 MM 0.0513 33.74682 10.96391 0.4698 4 2.170 MM 0.1303 3.26053 4.17021e-1 0.0454 Totals : 7183.10381 2403.52596 ===================================================================== *** End of Report ***HY-LCMS-02 6/29/2015 2:15:16 PM Li Shan(LCMS-02)Page 1 of 1

Data File D:\\AGLIENT 1260\\DATA\\20150629\\20150629 2015-06-29 09-33-24\\BIZ2015-629-DJL4.DSample Name: BIZ2015-629-DJL4=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 35Acq. Instrument : HY-LCMS-02 Location : P1-D-03Injection Date : 6/29/2015 1:49:17 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150629\\20150629 2015-06-29 09-33-24\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 6/29/2015 9:33:24 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\10-80A,15MIN(RP-HPLC).MLast changed : 6/29/2015 2:16:13 PM by Li Shan(LCMS-02) (modified after loading)Method Info : 10-80A,16MIN Catalog No : HY-B0688 Batch#16760 A-RP-132 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150629\\20150629 2015-06-29 09-33-24\\BIZ2015-629-DJL4.D) ES-API, Pos, Sca 1.67360000050000040000030000020000010000000.511.522.53min HY-LCMS-02 6/29/2015 2:16:15 PM Li Shan(LCMS-02)Page 1 of 2

Data File D:\\AGLIENT 1260\\DATA\\20150629\\20150629 2015-06-29 09-33-24\\BIZ2015-629-DJL4.DSample Name: BIZ2015-629-DJL4MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.673 2823067 519.10 I 497.10 I 250.00 I 249.05 I*MSD1 SPC, time=1.653:1.707 of D:\\AGLIENT 1260\\DATA\\20150629\\20150629 2015-06-29 09-33-24\\BIZ2015-629-DJL4.D ES-API,100806040 497.1 249.1Max: 2605760100200300400500600700m/z *** End of Report ***HY-LCMS-02 6/29/2015 2:16:15 PM Li Shan(LCMS-02) 251.020 519.1Page 2 of 2