MK-8745_LCMS_20863_MedChemExpress

MS Report File ..60630 2016-06-30 08-34-59\\BIZ2016-630-WJ5.D Tgt Mass (CHM): Injection Date : 30 Jun 16 12:31 pm +0800 Seq. Line : 49 Sample Name : BIZ2016-630-WJ5 Location : P1-A-03 Acq. Operator : Su Xiao Ying(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 3 ul Acq. Method : D:\\Aglient 1260\\Data\\20160630\\20160630 2016-06-30 08-34-59\\100-1000MS+3MIN- Analysis Method : D:\\AGLIENT 1260\\DATA\\20160630\\20160630 2016-06-30 08-34-59\\100-1000MS+3MIN- Catalog No : HY-13819 Batch#20863 Method Info : HY-365_5HO1RS,M,A-RP-108，210nm,23min*DAD1 B, Sig=214,4 Ref=off mAU150010001.4271.7461.8292.3672.5001.55850000.5*DAD1 C, Sig=254,4 Ref=off mAU30020011.51.55822.5min*1.8181.8391.3201.4791.74500.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 501500001000005000000.51 Ion 1, MSD1 1,Target Mass 0 +H Positive, EIC=0.7:1.7 0.050-0.050.5 Integration Results for DAD1 B, Sig=214,4 Ref=off-0.112.3512.6341001.51.57322.5min*1.522.5min1.522.5min RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.43 0.01 1.48 1.66 0.04 1.56 0.03 3568.37 1786.43 98.86 1.75 0.02 6.14 4.65 0.17 1.83 0.04 30.06 13.61 0.83 2.37 0.01 1.14 1.43 0.03 2.50 0.02 2.42 1.92 0.07 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.32 0.02 1.36 1.16 0.15 1.48 0.02 1.55 1.30 0.17 1.56 0.03 874.23 444.43 97.54 1.74 0.02 1.28 1.04 0.14 1.82 0.02 3.86 3.01 0.43 1.84 0.03 4.11 2.17 0.46 2.35 0.02 6.62 0.34 0.74 2.63 0.02 3.26 2.68 0.36HY-LCMS-02 6/30/2016 1:10:30 PM Su Xiao Ying(LCMS-02)Page 1 of 2

MS ReportRet. Time: 1.57 <<<< POSITIVE SPECTRA >>>> ES-API Positive200001750015000125001000075005000 217.4 217.6 434.1 282.0 435.0 433.0 216.625000 432.0200400600800m/zHY-LCMS-02 6/30/2016 1:10:30 PM Su Xiao Ying(LCMS-02)Page 2 of 2