_+_-JQ-1_NP-HPLC_18896_MedChemExpress

Data File D:\\CHEM\\DATA\\20151208\\20151208 2015-12-08 12-03-36\\014-0401.DSample Name: XWJ2980-005-1=====================================================================Acq. Operator : CSS(HPLC-10) Seq. Line : 4Acq. Instrument : Instrument 1 Location : Vial 14Injection Date : 2015-12-08 13:29:42 Inj : 1 Inj Volume : 5.000 µlAcq. Method : D:\\CHEM\\DATA\\20151208\\20151208 2015-12-08 12-03-36\\OD,95B-ETOH,254NM,C2.MLast changed : 2015-12-08 13:01:51 by CSS(HPLC-10) (modified after loading)Analysis Method : D:\\CHEM\\.M\\OZ,85-ETOH,210NM,C2.M Last changed : 2015-12-10 10:56:17 by CSS(HPLC-10) (modified after loading)Catalog No : HY-13030 Batch#18896 C-NP-16 Additional Info : Peak(s) manually integrated VWD1 A, Wavelength=254 nm (20151208\\20151208 2015-12-08 12-03-36\\014-0401.D) 12.468mAU600500400300200100005101520min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier: : 1.0000Dilution: : 1.0000Use Multiplier & Dilution Factor with ISTDs Signal 1: VWD1 A, Wavelength=254 nm Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 12.468 BB 0.4225 1.82721e4 661.03076 100.0000 Totals : 1.82721e4 661.03076 ===================================================================== *** End of Report ***Instrument 1 2015-12-10 10:57:44 CSS(HPLC-10)Page 1 of 1

Data File D:\\CHEM\\DATA\\20151208\\20151208 2015-12-08 12-03-36\\012-0301.DSample Name: XWJ2980-005-1_0=====================================================================Acq. Operator : CSS(HPLC-10) Seq. Line : 3Acq. Instrument : Instrument 1 Location : Vial 12Injection Date : 2015-12-08 13:03:17 Inj : 1 Inj Volume : 5.000 µlAcq. Method : D:\\CHEM\\DATA\\20151208\\20151208 2015-12-08 12-03-36\\OD,95B-ETOH,254NM,C2.MLast changed : 2015-12-08 13:01:51 by CSS(HPLC-10) (modified after loading)Analysis Method : D:\\CHEM\\.M\\OZ,85-ETOH,210NM,C2.M Last changed : 2015-12-10 10:58:45 by CSS(HPLC-10) (modified after loading)Catalog No : HY-13030 Batch#18896 C-NP-16 Additional Info : Peak(s) manually integrated VWD1 A, Wavelength=254 nm (20151208\\20151208 2015-12-08 12-03-36\\012-0301.D)mAU40302010005101520min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier: : 1.0000Dilution: : 1.0000Use Multiplier & Dilution Factor with ISTDs No peaks found ===================================================================== *** End of Report ***Instrument 1 2015-12-10 10:58:47 CSS(HPLC-10)Page 1 of 1

Data File D:\\CHEM\\DATA\\20151208\\20151208 2015-12-08 12-03-36\\077-0201.DSample Name: XWJ2980-005-1_RS=====================================================================Acq. Operator : CSS(HPLC-10) Seq. Line : 2Acq. Instrument : Instrument 1 Location : Vial 77Injection Date : 2015-12-08 12:36:15 Inj : 1 Inj Volume : 5.000 µlAcq. Method : D:\\CHEM\\DATA\\20151208\\20151208 2015-12-08 12-03-36\\OD,95B-ETOH,254NM,C2.MLast changed : 2015-12-08 13:01:51 by CSS(HPLC-10) (modified after loading)Analysis Method : D:\\CHEM\\.M\\OZ,85-ETOH,210NM,C2.M Last changed : 2015-12-10 10:56:17 by CSS(HPLC-10) (modified after loading)Catalog No : HY-13030 Batch#18896 C-NP-16 Additional Info : Peak(s) manually integrated VWD1 A, Wavelength=254 nm (20151208\\20151208 2015-12-08 12-03-36\\077-0201.D) 14.488 12.499mAU600500400300200100005101520min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier: : 1.0000Dilution: : 1.0000Use Multiplier & Dilution Factor with ISTDs Signal 1: VWD1 A, Wavelength=254 nm Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 12.499 BB 0.4193 9999.08887 365.31702 26.9522 2 14.488 BB 0.5778 2.71003e4 702.86102 73.0478 Totals : 3.70994e4 1068.17804 ===================================================================== *** End of Report ***Instrument 1 2015-12-10 10:56:44 CSS(HPLC-10)Page 1 of 1