Pitolisant_hydrochloride_LCMS_14715_MedChemExpress

Data File D:\\AGLIENT 1260\\DATA\\20150109\\20150109 2015-01-09 09-16-10\\BIZ2015-109-DJL12.DSample Name: BIZ2015-109-DJL12=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 65Acq. Instrument : HY-LCMS-02 Location : Vial 59Injection Date : 1/9/2015 2:45:19 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150109\\20150109 2015-01-09 09-16-10\\100-1000MS+3MIN( 0.02%FA).MLast changed : 1/9/2015 9:16:10 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20150108\\20150108 2015-01-08 09-25-26\\100-1000MS+3MIN( 0.02%FA).M (Sequence Method)Last changed : 1/9/2015 3:31:07 PM by Li Shan(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-102,40℃ Catalog No : HY-12199B Batch#14715 A-RP-32 Additional Info : Peak(s) manually integrated DAD1 B, Sig=214,4 Ref=off (D:\\AGLIENT...0\\DATA\\20150109\\20150109 2015-01-09 09-16-10\\BIZ2015-109-DJL12.D) 1.532mAU500400300200 1.98510000.511.522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 B, Sig=214,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.532 MM 0.0759 2699.94751 592.95709 99.7975 2 1.985 MM 0.0376 5.47908 2.43051 0.2025 Totals : 2705.42659 595.38760 ===================================================================== *** End of Report ***HY-LCMS-02 1/9/2015 3:31:09 PM Li Shan(LCMS-02)Page 1 of 1

Data File D:\\AGLIENT 1260\\DATA\\20150109\\20150109 2015-01-09 09-16-10\\BIZ2015-109-DJL12.DSample Name: BIZ2015-109-DJL12=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 65Acq. Instrument : HY-LCMS-02 Location : Vial 59Injection Date : 1/9/2015 2:45:19 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150109\\20150109 2015-01-09 09-16-10\\100-1000MS+3MIN( 0.02%FA).MLast changed : 1/9/2015 9:16:10 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20150108\\20150108 2015-01-08 09-25-26\\100-1000MS+3MIN( 0.02%FA).M (Sequence Method)Last changed : 1/9/2015 3:32:40 PM by Li Shan(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-102,40℃ Catalog No : HY-12199B Batch#14715 A-RP-32 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150109\\20150109 2015-01-09 09-16-10\\BIZ2015-109-DJL12.D) ES-API, Pos, Sca 1.5501200000100000080000060000040000020000000.511.522.53min HY-LCMS-02 1/9/2015 3:32:41 PM Li Shan(LCMS-02)Page 1 of 2

Data File D:\\AGLIENT 1260\\DATA\\20150109\\20150109 2015-01-09 09-16-10\\BIZ2015-109-DJL12.DSample Name: BIZ2015-109-DJL12MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.550 24741976 298.15 I 297.20 I 296.15 I*MSD1 SPC, time=1.507:1.744 of D:\\AGLIENT 1260\\DATA\\20150109\\20150109 2015-01-09 09-16-10\\BIZ2015-109-DJL12.D ES-API100806040200100200300400500600700800m/z 296.1Max: 628603 *** End of Report ***HY-LCMS-02 1/9/2015 3:32:41 PM Li Shan(LCMS-02) 299.2 298.1Page 2 of 2